| Course Unit Code | Course Unit Title | Type of Course Unit | Year of Study | Semester | Number of ECTS Credits | | KTY114 | Kimyada Ayırma Teknikleri | Elective | 1 | 2 | 6 |
|
| Level of Course Unit |
| Second Cycle |
| Objectives of the Course |
| The main objective of this course is to teach the basic principles of extraction, chromatographic and electrophoretic separation methods. |
| Name of Lecturer(s) |
| Dr.Öğr.Üyesi Bülent ŞENGÜL |
| Learning Outcomes |
| 1 | 1.At the end of the course the student will learn the basic principles of the extractions, chromatographic and electrophoretic separation methods. Theoretical and technical details of the instrumentation. |
|
| Mode of Delivery |
| Normal Education |
| Prerequisites and co-requisities |
| Retail |
| Recommended Optional Programme Components |
| No suggested poit |
| Course Contents |
| - Classification of Separation Methods
- Chemical Reactions and Separation
- Equilibrium, Partition Coefficients and Distribution Ratios
- Liquid-Liquid Extraction, Solid Phase Extraction
- Classification of Chromatographic Methods
- Theory and Equations
- Separation Performance; Gas and Liquid Mobile Phase Behaviour
- Optimization of Chromatographic Separations (chemical selectivity, resolution, instrumental performance and analysis time)
- Gas Chromatography
- Liquid Chromatography (normal phase, reverse phase)
- Ion Exchange Chromatography, Size Exclusion Chromatography
- Supercritical Fluid Chromatography
- Electrophoresis |
| Weekly Detailed Course Contents |
|
| 1 | Classification of Separation Methods, Chemical Reactions and Separation | | | | 2 | Equilibrium Approach (partitioning between phases) | | | | 3 | Partition Coefficients and Distribution Ratios | | | | 4 | Liquid-Liquid Extraction, Solid Phase Extraction | | | | 5 | Classification of Chromatographic Methods, Theory and Equations | | | | 6 | Solubility Parameters, Separation Performance; Gas and Liquid Mobile Phase Behaviour | | | | 7 | Optimization of Chromatographic Separations (chemical selectivity, resolution, instrumental performance and analysis time) | | | | 8 | Midterm exam | | | | 9 | Gas Chromatography | | | | 10 | Liquid Chromatography (normal phase, reverse phase) | | | | 11 | Ion Exchange Chromatography and Size Exclusion Chromatography | | | | 12 | Supercritical Fluid Chromatography | | | | 13 | Electrophoresis | | | | 14 | Dedectors | | | | 15 | injectors and column selection | | | | 16 | Final exam | | |
|
| Recommended or Required Reading |
| 1- James M. Miller (1975) Separation Methods in Chemical Analysis John Wiley, New York.
2- D.A. Skoog, F.J. Holler, T.A. Nieman (2007) Principles of Instrumental Analysis, 6 th Ed. Thomson Brooks/Cole, USA.
3- F. Rouessac, A. Rouessac (2000) Chemical Analysis Modern Instrumentation Methods and Techniques, John Wiley, London. |
| Planned Learning Activities and Teaching Methods |
|
| Assessment Methods and Criteria | |
| Midterm Examination | 1 | 100 | | SUM | 100 | |
| Final Examination | 1 | 100 | | SUM | 100 | | Term (or Year) Learning Activities | 40 | | End Of Term (or Year) Learning Activities | 60 | | SUM | 100 |
| | Language of Instruction | | Turkish | | Work Placement(s) | | No internship |
|
| Workload Calculation |
|
| Midterm Examination | 1 | 2 | 2 |
| Final Examination | 1 | 2 | 2 |
| Criticising Paper | 5 | 5 | 25 |
| Self Study | 2 | 20 | 40 |
| Individual Study for Homework Problems | 3 | 12 | 36 |
| Individual Study for Mid term Examination | 1 | 15 | 15 |
| Individual Study for Final Examination | 2 | 30 | 60 |
|
| Contribution of Learning Outcomes to Programme Outcomes |
|
| * Contribution Level : 1 Very low 2 Low 3 Medium 4 High 5 Very High |
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